3,4-Dichlorophenol → HCID 66825883, compound

HRID 2359976Notes

Reaction equation

HRID 2359976 reaction equation
Cl[C:2]1[N:6]([CH3:7])[N:5]=[C:4]([CH:8]([F:10])[F:9])[C:3]=1[CH:11]=[O:12].[Cl:13][C:14]1[CH:15]=[C:16]([OH:21])[CH:17]=[CH:18][C:19]=1[Cl:20].C(=O)([O-])[O-:23].[K+].[K+]>>[Cl:13][C:14]1[CH:15]=[C:16]([CH:17]=[CH:18][C:19]=1[Cl:20])[O:21][C:2]1[N:6]([CH3:7])[N:5]=[C:4]([CH:8]([F:10])[F:9])[C:3]=1[C:11]([OH:12])=[O:23]

Participants

4

Reactant 3

HCID 72583,4-DichlorophenolHCID 11430Potassium CarbonateHCID 197546925-Chloro-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carbaldehyde

Product 1

HCID 66825883HCID 66825883, compound

Procedure

The title compound was prepared using 5-chloro-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carbaldehyde and 3,4-dichlorophenol in the manner similar to the method in Production Example 1 above except potassium carbonate was used instead of potassium hydroxide.

Sources & evidence

ORD record
ord-063566a7b26e4224abea9bb811b7c032
Source dataset
uspto-grants-2014_04
Patent number
US08686018B2

Reaction notes

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