HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylamine → HCID 13391417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | HCID 12683883 | HCID 12683883 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13391417 | HCID 13391417 | — |
Reaction Steps
A mixture of the product of Procedure 46, 1.0 g. (0.0025 mole) and 0.37 g. (0.005 mole) of 2-methylpropylamine in 20 ml. of ethanol is refluxed for 16 hrs. The desired product precipitated as the hydrobromide salt which was collected and mixed with dilute aqueous sodium hydroxide to convert it into the free base form, m.p. 185°-187°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642345 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-0468be095c154520a93013c08303dabd |
| Source note | uspto-grants-1987_02 |