HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Tartaric acid → HCID 86658826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Tartaric acid | HCID 439655 | — |
| Reactant | Sunitinib | HCID 5329102 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86658826 | HCID 86658826 | — |
Reaction Steps
Sunitinib (2.20, 5.52 mmol) was suspended in methanol (100 ml). 0.83 g of D-tartaric acid was added. Mixture was heated until all material was dissolved, then left to cool to room temperature to form crystalline sunitinib D-tartrate, 2.95 g. Melting point 183-187° C. (form II)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686023B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-42a52ecb3f3e41d9a8bb3131903005c5 |
| Source note | uspto-grants-2014_04 |