HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Tartaric acid → HCID 86658827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Tartaric acid | HCID 444305 | — |
| Reactant | Sunitinib | HCID 5329102 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86658827 | HCID 86658827 | — |
Reaction Steps
Sunitinib (2.15, 5.40 mmol) was suspended in methanol (100 ml). 0.81 g of L-tartaric acid was added. Mixture was heated until all material was dissolved, then left to cool to room temperature to form crystalline sunitinib L-tartrate, 2.1 g. Melting point: 189-193° C. (form II)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686023B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-1b73067c00b44db990fcd6a7fd8c9327 |
| Source note | uspto-grants-2014_04 |