Citric Acid → HCID 86658825, compound

Participants

Reaction Steps

Sunitinib (1.45 g, 3.64 mmol) was dissolved in boiling ethanol (140 ml), then citric acid (0.23 g, 1.21 mmol) was added to the solution, which was left to cool to room temperature to give sunitinib citrate with melting points 166-170° C. (Form I) and 219-224° C. (Form III).

Provenance & Evidence