Methane → HCID 20217713, compound

HRID 236009Notes

Reaction equation

HRID 236009 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][NH:9][C:10]2[N:11]([CH2:23][CH:24]([CH3:26])[CH3:25])[C:12]3[N:13]([CH2:20][CH2:21][N:22]=3)[C:14](=[O:19])[C:15]=2[NH:16][CH:17]=O)=[CH:4][CH:3]=1.[OH-].[Na+].C>O>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][N:9]2[CH:17]=[N:16][C:15]3[C:14](=[O:19])[N:13]4[CH2:20][CH2:21][N:22]=[C:12]4[N:11]([CH2:23][CH:24]([CH3:26])[CH3:25])[C:10]2=3)=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 297MethaneHCID 14798Sodium HydroxideHCID 20217710HCID 20217710, compound

Product 1

HCID 20217713HCID 20217713, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The formyl amino compound of Procedure 88 (0.08 mol) is dissolved with warming in a solution of sodium hydroxide (0.09 mol) in 100 ml. water. The solution is treated with activated charcoal, filtered, and the filtrate neutralized with acetic acid. The precipitate is collected.

Workup

  1. filtrationfiltered
  2. customThe precipitate is collected

Sources & evidence

ORD record
ord-9156d82815ba4630893f24f70b9dd434
Source dataset
uspto-grants-1987_02
Patent number
US04642345

Reaction notes

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