HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 528718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 2-Methyl-2-butanol | HCID 6405 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | Propionic anhydride | HCID 31263 | — |
| Reactant | Pyrylium | HCID 9548819 | — |
| Product | HCID 528718 | HCID 528718 | — |
| Product | Pyridine, 2,4,6-triethyl- | HCID 3084917 | — |
Reaction Steps
The procedure of Example 1-a was repeated for this synthesis. From 0.05 mole (5.4 ml) of 2-methyl-2-butanol, 0.1 mole (6.5 ml) of methanesulfonic acid and 0.4 mole of propionic anhydride, after treating with NH4OH the aqueous solution of pyrylium salts, 4.1 g (50%) were obtained of a mixture of 2,6-diethyl-3,4-dimethylpyridine and of 2,4,6-triethylpyridine in the respective proportions of 96% and 4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642359 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-530db13112be4063a39ebc104a0a74b6 |
| Source note | uspto-grants-1987_02 |