P-Cresol → Trimethyl(4-methylphenoxy)silane

HRID 236026Notes

Reaction equation

HRID 236026 reaction equation
[CH3:1][Si:2]([CH3:5])([CH3:4])Cl.[CH:6]1[C:11]([OH:12])=[CH:10][CH:9]=[C:8]([CH3:13])[CH:7]=1>>[CH3:1][Si:2]([CH3:5])([CH3:4])[O:12][C:11]1[CH:6]=[CH:7][C:8]([CH3:13])=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 2879P-CresolHCID 6397Chlorotrimethylsilane

Product 1

HCID 286939Trimethyl(4-methylphenoxy)silane

Procedure

The procedure of Example 2 was perfomred with 40 moles each of trimethylchlorosilane and p-cresol. The reactor temperature went to about 122° C. About 7.2 kg/h of trimethyl-p-cresyloxysilane was produced. B.p. 198° C., D.4/20 0.9183.

Workup

  1. customwent to about 122° C

Sources & evidence

ORD record
ord-edc763d9c98343868b81ed84f6904415
Source dataset
uspto-grants-1987_02
Patent number
US04642363

Reaction notes

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