1-Decene → 4-Decylbenzaldehyde

HRID 2360343Notes

Reaction equation

HRID 2360343 reaction equation
[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].Br[C:12]1[CH:19]=[CH:18][C:15]([CH:16]=[O:17])=[CH:14][CH:13]=1>>[CH2:1]([C:12]1[CH:19]=[CH:18][C:15]([CH:16]=[O:17])=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 133811-DeceneHCID 707414-Bromobenzaldehyde

Product 1

HCID 128390194-DecylbenzaldehydeYield 94.4%

Procedure

General procedure G was used to couple 1-decene (8.1 mmol) to 4-bromobenzaldehyde (5.4 mmol) to yield 1.25 g (5.1 mmol) of the title product after column chromatography. Spectral data was consistent with previously reported compounds.

Sources & evidence

ORD record
ord-fe15578b6394480597ecfcc87dc22db1
Source dataset
uspto-grants-2014_04
Patent number
US08686046B2

Reaction notes

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