HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 46314623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 4-Bromo-2,6-difluoroaniline | HCID 610191 | — |
| Product | HCID 46314623 | HCID 46314623 | 81.4% |
Reaction Steps
The title compound (0.401 g) was prepared from 2,6-difluoro-4-bromo aniline (0.5 g, 2.4 mmol) and phenylboronic acid (0.38 g, 3.12 mmol) as a white solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.60 (d, J 7.4, 2H), 7.38 (t, J 7.5, 2H), 7.30-7.25 (m, 3H), 5.33 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-1f068def37344b3d8c555d7ce34d5ac4 |
| Source note | uspto-grants-2014_04 |