HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,6-dichloroaniline → HCID 66997456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,6-dichloroaniline | HCID 69680 | — |
| Reactant | 2-Chlorophenylboronic acid | HCID 2734322 | — |
| Product | HCID 66997456 | HCID 66997456 | 69.9% |
Reaction Steps
The title compound (0.4 g) was prepared from 4-bromo-2,6-dichloroaniline (0.5 g, 2.1 mmol) and 2-chlorophenylboronic acid (0.421 g, 2.7 mmol) as a white solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.55-7.50 (m, 1H), 7.40-7.32 (m, 3H), 7.29 (s, 2H), 5.72 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-9a21214b289b487c880f76a26f7f6e30 |
| Source note | uspto-grants-2014_04 |