HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-5-methoxyphenylboronic acid → HCID 66996748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-5-methoxyphenylboronic acid | HCID 4157211 | — |
| Reactant | 4-Bromo-2-chloro-6-fluoroaniline | HCID 20434620 | — |
| Product | HCID 66996748 | HCID 66996748 | 59% |
Reaction Steps
The title compound (70 mg) was prepared from 4-bromo-2-chloro-6-fluoroaniline (100 mg, 0.44 mmol) and 2-fluoro-5-methoxyphenylboronic acid (98 mg, 0.58 mmol) as a white solid. 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 7.30-7.24 (m, 2H), 7.17 (t, J 9.1, 1H), 7.02-6.97 (m, 1H), 6.90-6.84 (m, 1H), 5.61 (s, 2H), 3.77 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08686048B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-bec2e9434bb8472580a9815e146f83cf |
| Source note | uspto-grants-2014_04 |