HRID2360503

反应详情

EQUATION

反应方程式

HRID 2360503 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2.7 g methyl 5-tert-butyl-2-methoxy-3-nitro-benzoate are dissolved in 120 ml of methanol, combined with 270 mg of 10% palladium on charcoal and hydrogenated for 12 hours at ambient temperature and 4 bar hydrogen pressure. Then the catalyst is filtered off, the solvents are eliminated in vacuo and the residue thus obtained is further reacted directly.

WORKUP

后处理

  1. filtrationThen the catalyst is filtered off
  2. customthe residue thus obtained
  3. customis further reacted directly