HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2360594Generated: November 3, 2026
Methyl Methanesulfonate → HCID 178505332, compound
https://huagongshe.com/reaction/2360594
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Methanesulfonate | HCID 4156 | — |
| Reactant | Scopine-2,2-dithienyl glycolate | HCID 29927228 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178505332 | HCID 178505332 | — |
Reaction Steps
75.5 g scopine di-(2-thienyl)glycolate are dissolved in 750 ml acetonitrile while heating gently. After the addition of 22 ml of methyl methanesulphonate the mixture is stirred at 55° C. After the reaction has ended about 350 ml solvent distilled off under reduced pressure. The product crystallises out and is filtered off. It is purified by recrystallisation from methanol/acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08686148B2 |
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| Source dataset | uspto-grants-2014_04 |
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| ORD ID | ord-7e863d57f0b04fa2991affecf8a4e66f |
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| Source note | uspto-grants-2014_04 |
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