HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenylthiocyclohexanone Oxime → HCID 20217891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenylthiocyclohexanone Oxime | HCID 20217861 | — |
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20217891 | HCID 20217891 | — |
Reaction Steps
Following an analogous procedure to that of Sasatani, S. et al. described in Tetrahedron Letters, Vol. 24 (No. 43), pp 4711-4712 (1982), 4-phenylthiocyclohexanone oxime is reacted with diisobutyl aluminum hydride in methylene chloride to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04642348 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-003f739b4cc34785830a189acfed03aa |
| Source note | uspto-grants-1987_02 |