HRID236114

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8459

N,N-Bis(1-methylethyl)-1,2-ethanediamine

C8H20N2

HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

HCID13607983

未命名化合物

PRODUCTS

生成物

结构：CC(C)N(CCNC(=O)N1CCCC(S(=O)(=O)c2ccccc2)C1)C(C)C

HCID13608029

未命名化合物

收率 59.8%

PROCEDURE

实验过程

Following the procedure of Example 16, diisopropylaminoethylamine and 1,1'-carbonyldiimidazole and 3-(phenylsulfonyl)piperidine were reacted to give the title compound which was crystallized from diethyl ether-hexane as white solid in 59.8% yield, m.p. 82.5°-84° C.

WORKUP

后处理

customwere reacted