HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 13022013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13022013 | HCID 13022013 | 84% |
Reaction Steps
Ethyl 2-bromopropionate (0.125 moles) was diluted with 75 ml of toluene, and morpholine (0.3 moles) was added thereto, followed by stirring for 10 hours at room temperature. White solid was removed by filtration, and then the filtrate was distilled to obtain 2-morpholinopropionic acid ethyl ester (0.105 moles).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691352B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-f039bb4953434af6b361ba1ca223d5b4 |
| Source note | uspto-grants-2014_04 |