HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → Diethylamino propionic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Product | Diethylamino propionic acid ethyl ester | HCID 13010788 | 80% |
Reaction Steps
To ethyl 2-bromopropionate (0.15 moles), diethylamine (0.4 moles) was added, followed by stirring for 10 hours at room temperature. White solid was removed by filtration, and then the filtrate was distilled to obtain 2-diethylaminopropionic acid ethyl ester (0.120 moles).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691352B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-6d391d24a9ee4ac98d7bf64f866fe158 |
| Source note | uspto-grants-2014_04 |