HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxyphenyldiphenylsulfonium 4-methylbenzenesulfonate → 4-Hydroxyphenyldiphenylsulfonium 1,1,3,3,3-pentafluoro-2-(methacryloyloxy)propane-1-sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxyphenyldiphenylsulfonium 4-methylbenzenesulfonate | HCID 22389781 | — |
| Reactant | Triethylammonium 1,1,3,3,3-pentafluoro-2-(methacryloyloxy)propane-1-sulfonate | HCID 86656197 | — |
| Solvent | Water methylene chloride | HCID 21908982 | — |
| Product | 4-Hydroxyphenyldiphenylsulfonium 1,1,3,3,3-pentafluoro-2-(methacryloyloxy)propane-1-sulfonate | HCID 86656198 | — |
Reaction Steps
4-hydroxyphenyldiphenylsulfonium 4-methylbenzenesulfonate and triethylammonium 1,1,3,3,3-pentafluoro-2-(methacryloyloxy)propane-1-sulfonate of Synthesis Example 1-2 are mixed and ion-changed in a dichloromethane-water system. An organic layer after washing by water was concentrated under reduced pressure and was used for the next reaction as a crude substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691490B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-60df5302d4704d9a9c671255a6400603 |
| Source note | uspto-grants-2014_04 |