HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58243400, compound → HCID 58243433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58243400 | HCID 58243400 | — |
| Reactant | HCID 58243429 | HCID 58243429 | — |
| Product | HCID 58243433 | HCID 58243433 | — |
Reaction Steps
In a similar fashion (Route 20, GP I), 1-{[4-(1-methylethyl)-1,4-diazepan-1-yl]carbonyl}azetidin-3-ol (100 mg, 0.41 mmol) and 2-(5-fluoropyridin-2-yl)propan-2-ol (90 mg, 0.41 mmol) were used to give the title compound. Crude material (50 mg) after workup gave the title compound as colourless oil (17.7 mg) after purification by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691804B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-f4b5e8daa5754155b62f02c4d3efcccd |
| Source note | uspto-grants-2014_04 |