HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 66719151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 66823510 | HCID 66823510 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66719151 | HCID 66719151 | — |
Reaction Steps
To the solution of 9-5 (60 mg, 0.1 mmol) in 1 mL of DCM was added TFA (1 mL) and the mixture was stirred at room temperature for 3 h. The mixture was concentrated by evaporation and the residue was purified by prep.HPLC to give the product 9-6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691825B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-05d0f7714d27445389071569ca4fe9f8 |
| Source note | uspto-grants-2014_04 |