HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86673423, compound → HCID 86673426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86673423 | HCID 86673423 | — |
| Reactant | HCID 86673424 | HCID 86673424 | — |
| Product | HCID 86673426 | HCID 86673426 | — |
Reaction Steps
Prepared according to the same procedure as diethyl 2,5-difluorobenzylphosphonate, starting with 2-bromo-4-(bromomethyl)pyrimidine. 1H NMR (500 MHz, DMSO-d6) δ 8.69-8.58 (m, 1H), 7.67-7.44 (m, 1H), 4.14-3.91 (m, 4H), 3.62-3.43 (m, 2H), 1.42-1.09 (m, 6H), Mass spec.: 310.1 (MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691821B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-782ddab5fabb4191987ea9fb3990eada |
| Source note | uspto-grants-2014_04 |