HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiopheneacetyl chloride → HCID 67251903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiopheneacetyl chloride | HCID 162362 | — |
| Reactant | (S)-N-(8-methoxytetralin-2-yl)-N-propylamine | HCID 12741415 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 67251903 | HCID 67251903 | — |
Reaction Steps
Synthesis worked according to the preparation of A4-1 when using 310 mg (1.4 mmol) enantiomerical pure (S)-N-(8-methoxytetralin-2-yl)-N-propylamine ((R)-A2-1: R=OMe) and 0.35 mL (2.8 mmol) 2-thienyl acetic acid chloride. Flash chromatography was done with hexane/ethyl acetate 20/1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691839B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-5ac66632c3d248888d79fe9889b499c4 |
| Source note | uspto-grants-2014_04 |