HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 140570811, compound → HCID 136351076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 140570811 | HCID 140570811 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 136351076 | HCID 136351076 | — |
Reaction Steps
A solution of Example 22C (0.084 g, 0.136 mmol) in toluene (3 mL) was heated to 110° C. for 10 hours. The reaction was cooled to ambient temperature and concentrated to give the title compound, which was used without further purification. MS ESI(+) m/z 601.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691810B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-72af7e1f0e4c4b4592bba64c89469f50 |
| Source note | uspto-grants-2014_04 |