Water → HCID 136379490, compound

Participants

Reaction Steps

A solution of Example 46D (0.66 g, 0.107 mmol) in 1-methyl-2-pyrrolidinone (1.2 mL) was heated at 110° C. for 5 hours. The reaction was cooled to ambient temperature and poured into water (5 mL). The resulting suspension was filtered, and the solid collected was washed with water and dried under vacuum to provide the title compound. MS ESI(+) m/z 601.2 [M+H]+.

Provenance & Evidence