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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2362813Generated: October 28, 2026

Hydrochloric Acid → HCID 178510543, compound

https://huagongshe.com/reaction/2362813

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantSodium SulfideHCID 14804—
ReactantHCID 57452402HCID 57452402—
SolventDimethylformamideHCID 6228—
ProductHCID 178510543HCID 178510543—

Reaction Conditions

Temperature80 °C

Reaction Steps

0.30 g (0.70 mmol) of the compound from Example 31A is dissolved in 2 ml of DMF, and 0.19 g (2.43 mmol) of sodium sulphide is added. The mixture is stirred at 80° C. for 2 h and then at RT for 12 h. 1N hydrochloric acid (10 ml) is then added, and the precipitate is filtered off.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08691850B2
Source datasetuspto-grants-2014_04
ORD IDord-bc8f7d9f1b3c4fceaf8d71579fe2935d
Source noteuspto-grants-2014_04