HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2362841Generated: October 27, 2026
Ethanol → 3-Aminocinnamaldehyde thiosemicarbazone
https://huagongshe.com/reaction/2362841
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 3-nitrocinnamaldehyde Thiosemicarbazone | HCID 86633306 | — |
| Solvent | HCID 178506451 | HCID 178506451 | — |
| Product | 3-Aminocinnamaldehyde thiosemicarbazone | HCID 86633312 | 68% |
Reaction Steps
A solution of 10 mL ethanol and 2 mL sodium carbonate 2N is saturated in hydrogen sulfur. 500 mg (2 mmoles) 3-nitrocinnamaldehyde thiosemicarbazone prepared in step 2A are added. The solution is heated 10 minutes at 50° C., then 3 minutes at 75° C. The solution is cooled in a ice bath. The crystals formed are filtered, washed with ethanol. 299 mg of 3-aminocinnamaldehyde thiosemicarbazone is obtained. Yield 68%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08691854B2 |
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| Source dataset | uspto-grants-2014_04 |
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| ORD ID | ord-2b3ffdbaa05f4d00ae32bf4da88b8ea2 |
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| Source note | uspto-grants-2014_04 |
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