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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 236301Generated: October 30, 2026

Hydrochloric Acid → HCID 53832834, compound

https://huagongshe.com/reaction/236301

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 17785308HCID 17785308—
ReactantSodium NitriteHCID 23668193—
SolventDimethyl SulfoxideHCID 679—
SolventWaterHCID 962—
ProductHCID 53832834HCID 53832834—

Reaction Conditions

Temperature50 °C

Reaction Steps

To a solution of 7.0 g of XXVI in 50 ml of DMSO was added 8 ml of 5N HCl and 2.7 g of NaNO2 dissolved in 5 ml of water. The reaction mixture was stirred 10 minutes at 50° C. and then 100 ml of water was added. The red crystals were filtered off. Yield 6 g (XXVII).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04644001
Source datasetuspto-grants-1987_02
ORD IDord-122f69a11ca74354995043e0492f2395
Source noteuspto-grants-1987_02