HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 20217052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 54485518 | HCID 54485518 | — |
| Product | HCID 20217052 | HCID 20217052 | — |
Reaction Steps
A solution of 2.2 g of 1-cyclobutyl-5,6-diamino-2,4-(1H,3H)-pyrimidinedione (X) in 10 ml of acetic acid was refluxed for 2 hours. The solution was evaporated. The received oil was refluxed in 30 ml of 5N NaOH for 1 hour and then neutralized with 5N HCl. The crystals were filtered off and recrystallized from 100 ml ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04644001 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-98325eadf8054070ae3b6d33d054799b |
| Source note | uspto-grants-1987_02 |