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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2363264Generated: October 29, 2026

Diethyl Ether → HCID 86682254, compound

https://huagongshe.com/reaction/2363264

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
ReactantIsobutanolHCID 6560—
ReactantOxalyl chlorideHCID 65578—
ProductHCID 86682254HCID 86682254—

Reaction Steps

Chloro-oxo-acetic acid isobutyl ester was prepared by adding oxalyl chloride (21 μL, 252 μmol) to a solution of isobutanol (21 μL, 226 μmol) in ether (206 μL, 2.0 mmol). The mixture was stirred at room temperature for 15 min and then evaporated.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08691868B2
Source datasetuspto-grants-2014_04
ORD IDord-d9fd6006f5ba45fea3b5391d3ce9e727
Source noteuspto-grants-2014_04