Diethyl Ether → HCID 86682254, compound

HRID 2363264Notes

Reaction equation

HRID 2363264 reaction equation
[C:1](Cl)(=[O:5])[C:2]([Cl:4])=[O:3].[CH2:7]([OH:11])[CH:8]([CH3:10])[CH3:9].CCOCC>>[CH2:7]([O:11][C:1](=[O:5])[C:2]([Cl:4])=[O:3])[CH:8]([CH3:10])[CH3:9]

Participants

4

Reactant 3

HCID 3283Diethyl EtherHCID 6560IsobutanolHCID 65578Oxalyl chloride

Product 1

HCID 86682254HCID 86682254, compound

Procedure

Chloro-oxo-acetic acid isobutyl ester was prepared by adding oxalyl chloride (21 μL, 252 μmol) to a solution of isobutanol (21 μL, 226 μmol) in ether (206 μL, 2.0 mmol). The mixture was stirred at room temperature for 15 min and then evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-d9fd6006f5ba45fea3b5391d3ce9e727
Source dataset
uspto-grants-2014_04
Patent number
US08691868B2

Reaction notes

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