HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → Chloromethyl 2-cyanoethylether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | Methylthiomethyl 2-cyanoethylether | HCID 86616732 | — |
| Product | Chloromethyl 2-cyanoethylether | HCID 86616731 | — |
Reaction Steps
Methylthiomethyl 2-cyanoethylether (3.3 g, 25 mmol) was dissolved in 70 mL of methylene chloride, and 2 mL of sulfuryl chloride (25 mmol) was added dropwise, and the reaction was further performed at room temperature for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08691970B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-9eef10283fa44218be2307d7308f4d43 |
| Source note | uspto-grants-2014_04 |