Hydrochloric Acid → HCID 70400181, compound

Participants

Reaction Steps

52.1 g of 35% hydrochloric acid and 13.4 g of water were added to 69.6 g (0.5 mol) of N-cyclohexylallylamine under cooling to maintain the temperature below 20° C. to obtain a 65.0% aqueous solution of N-cyclohexylallylamine hydrochloride (hereinafter abbreviated as CHAA.HCl). This solution was added with 2.64 g of initiator 1 and polymerized at 60° C. for 48 hours after the manner of Example 1, followed by the same treatment as in Example 1 to obtain 79.0 g of white powder (conversion: 89.9%).

Provenance & Evidence