Hydrochloric Acid → HCID 70400181, compound

HRID 236384Notes

Reaction equation

HRID 236384 reaction equation
[ClH:1].[CH:2]1([CH:8]=[CH:9][CH2:10][NH2:11])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1>O>[ClH:1].[CH:2]1([CH:8]=[CH:9][CH2:10][NH2:11])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 54463750HCID 54463750, compound

Product 1

HCID 70400181HCID 70400181, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

52.1 g of 35% hydrochloric acid and 13.4 g of water were added to 69.6 g (0.5 mol) of N-cyclohexylallylamine under cooling to maintain the temperature below 20° C. to obtain a 65.0% aqueous solution of N-cyclohexylallylamine hydrochloride (hereinafter abbreviated as CHAA.HCl). This solution was added with 2.64 g of initiator 1 and polymerized at 60° C. for 48 hours after the manner of Example 1, followed by the same treatment as in Example 1 to obtain 79.0 g of white powder (conversion: 89.9%).

Workup

  1. temperatureunder cooling
  2. temperatureto maintain the temperature below 20° C.

Sources & evidence

ORD record
ord-850f5bb12b0c468f8cb82bda36563747
Source dataset
uspto-grants-1987_02
Patent number
US04644042

Reaction notes

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