HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Diisopropylamino-acetic acid hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11333389 | HCID 11333389 | — |
| Solvent | Water | HCID 962 | — |
| Product | Diisopropylamino-acetic acid hydrochloride | HCID 46735981 | — |
Reaction Steps
5.4 g (25 mMol) diisopropylamino-acetic acid tert-butylester 2 was stirred with 6.25 ml (75 mMol) 12 M HCl in 25 ml water for 2.5 h at 60° C. After distillation in vacuo of water and excess of HCl, the residue was dried with toluene azeotropically.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697604B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-ebb2f625df644252aacb55878745cfe1 |
| Source note | uspto-grants-2014_04 |