HuagongsheHuagongshe Chemistry Print Report · For research reference only
Palmitoyl chloride → dibenzyl N-(N-hexadecanoyl-L-valyl)-L-glutamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Palmitoyl chloride | HCID 8206 | — |
| Reactant | dibenzyl N-(N-tert-butoxycarbonyl-L-valyl)glutamate | HCID 54081958 | — |
| Product | dibenzyl N-(N-hexadecanoyl-L-valyl)-L-glutamate | HCID 53989800 | 63.4% |
Reaction Steps
Starting from dibenzyl N-(N-tert-butoxycarbonyl-L-valyl)-L-glutamate (1 g) and hexadecanoyl chloride (620 mg), dibenzyl N-(N-hexadecanoyl-L-valyl)-L-glutamate (800 mg) was obtained as crystals according to a similar manner to that of Example 24.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04643990 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-9536b881da8e425a9b09543e05f20054 |
| Source note | uspto-grants-1987_02 |