HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,3,6-Tetrahydropyridine → HCID 20216140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,3,6-Tetrahydropyridine | HCID 12750 | — |
| Reactant | 3,4-Diacetoxybenzaldehyde | HCID 1517488 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20216140 | HCID 20216140 | — |
Reaction Steps
Using a similar procedure to that described in Example 7, but starting from 3,4-diacetoxybenzaldehyde (18.6 g.) and 1,2,3,6-tetrahydropyridine (13.9 g.) in methanol (150 ml.), there was obtained 1-(3,4-dihydroxybenzyl)-1,2,3,6-tetrahydropyridine as the free base (0.45 g.), m.p. >300° C.; microanalysis,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04645771 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-80cde4cb5b434134b99d802eb6ee0928 |
| Source note | uspto-grants-1987_02 |