HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 20216114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 1-(4-Hydroxybenzyl)-1,2,3,6-tetrahydropyridine | HCID 20216094 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20216114 | HCID 20216114 | — |
Reaction Steps
Aqueous hydrobromic acid (48% w/w) was added dropwise, with stirring, to a solution of 1-(4-hydroxybenzyl)-1,2,3,6-tetrahydropyridine (4.0 g.) in acetone (50 ml.) until no further precipitate was obtained. The solid was collected by filtration and recrystallised from ethanol to give 1-(4-hydroxybenzyl)-1,2,3,6-tetrahydropyridine hydrobromide (Example 18) (2.9 g.), m.p. 187°-190° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04645771 |
| Source dataset | uspto-grants-1987_02 |
| ORD ID | ord-03b8b3cfebe4412193a49d5ec1eff538 |
| Source note | uspto-grants-1987_02 |