Hydrochloric Acid → HCID 18966311, compound

HRID 236563Notes

Reaction equation

HRID 236563 reaction equation
C(OC([NH:8][CH:9]([CH2:20][CH:21]([CH3:23])[CH3:22])[CH:10]([OH:19])[CH2:11][S:12][CH:13]1[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1)=O)(C)(C)C.[ClH:24]>CO>[ClH:24].[NH2:8][CH:9]([CH2:20][CH:21]([CH3:23])[CH3:22])[CH:10]([OH:19])[CH2:11][S:12][CH:13]1[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 13893088HCID 13893088, compound

Product 1

HCID 18966311HCID 18966311, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a stirred solution of approximately 0.25 mmol of the resultant compound of Example 3 in methanol was added methanolic HCl (10 ml of approximately 0.75M). After 8-12 hours, the solvent was evaporated, and the desired compound was used without further purification.

Workup

  1. customthe solvent was evaporated
  2. customthe desired compound was used without further purification

Sources & evidence

ORD record
ord-1efaaebe0612424599b9001debfc936c
Source dataset
uspto-grants-1987_02
Patent number
US04645759

Reaction notes

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