Potassium Carbonate → HCID 67422374, compound

HRID 2365911Notes

Reaction equation

HRID 2365911 reaction equation
C(=O)([O-])[O-].[K+].[K+].[CH2:7]([O:9][C:10]([N:12]1[CH2:17][CH2:16][C:15]([C:19]2[CH:24]=[CH:23][C:22]([O:25][CH2:26][C:27]3[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=3)=[CH:21][C:20]=2[O:33][CH2:34][C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)(O)[CH2:14][CH2:13]1)=[O:11])[CH3:8]>C(C(C)=O)C>[CH2:7]([O:9][C:10]([N:12]1[CH2:17][CH2:16][CH:15]([C:19]2[CH:24]=[CH:23][C:22]([O:25][CH2:26][C:27]3[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=3)=[CH:21][C:20]=2[O:33][CH2:34][C:35]2[CH:36]=[CH:37][CH:38]=[CH:39][CH:40]=2)[CH2:14][CH2:13]1)=[O:11])[CH3:8]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 67423169HCID 67423169, compound

Product 1

HCID 67422374HCID 67422374, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

In a 100 ml round-bottomed flask, 9.7 g of potassium carbonate are added in small portions to a solution of 6.2 g of 4-(2,4-dihydroxyphenyl)piperidine-1-carboxylic acid ethyl ester (Example 10) in 62 ml of methyl ethyl ketone.

Sources & evidence

ORD record
ord-3748cf7d6c864c29b84f5e57571d9215
Source dataset
uspto-grants-2014_04
Patent number
US08697726B2

Reaction notes

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