huagongshe.com
HRID2366454

反应详情

EQUATION

反应方程式

HRID 2366454 的结构方程式

REACTANTS

反应物

2
结构：O=C1CCC(=O)N1Cl
HCID31398

N-Chlorosuccinimide

C4H4ClNO2

结构：NC(=O)c1cccc([N+](=O)[O-])c1N
HCID10797476

2-amino-3-nitrobenzamide

C7H7N3O3

PRODUCTS

生成物

1
结构：NC(=O)c1cc(Cl)cc([N+](=O)[O-])c1N
HCID25193320

2-Amino-5-chloro-3-nitrobenzamide

C7H6ClN3O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

A solution of 2-amino-3-nitrobenzamide (5 g) in acetonitrile (1250 mL) at 60° C. was treated with N-chlorosuccinimide (3.87 g), stirred for 24 hours, cooled and filtered.

WORKUP

后处理

  1. temperaturecooled
  2. filtrationfiltered