HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → 2-Amino-5-chloro-3-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 2-Amino-3-nitrobenzamide | HCID 10797476 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2-Amino-5-chloro-3-nitrobenzamide | HCID 25193320 | — |
Reaction Steps
A solution of 2-amino-3-nitrobenzamide (5 g) in acetonitrile (1250 mL) at 60° C. was treated with N-chlorosuccinimide (3.87 g), stirred for 24 hours, cooled and filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697736B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-dd286cf075b643649ecbec504a961aa7 |
| Source note | uspto-grants-2014_04 |