HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25193405, compound → 934162-32-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25193405 | HCID 25193405 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 934162-32-0 | HCID 25194665 | — |
Reaction Steps
To a solution of EXAMPLE 45C (11.2 g) in a mixture of THF (50 mL) and ethanol (50 mL) was added Raney nickel (50% in water, 11.0 g). The mixture was stirred under hydrogen (60 psi) for 5 hours. Solid material was filtered off and the filtrate was concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697736B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-61ea365c9aeb475584ace8a60f91860c |
| Source note | uspto-grants-2014_04 |