HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentene → HCID 91256749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentene | HCID 8882 | — |
| Reactant | Heptane | HCID 8900 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 91274444 | HCID 91274444 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 91256749 | HCID 91256749 | — |
Reaction Steps
Compound 7 (237.4 mg, 560 μmol) was dissolved in dry CH2Cl2 (2 mL), and bromine (32 μl, 620 μmol) was added. The reaction was monitored by TLC (heptane:EtOAc, 1:1). When the reaction was complete, a small amount of cyclopentene was added to the reaction mixture to remove the rests of Br2. The mixture was concentrated under reduced pressure and purified by quick Flash chromatography (Eluyent: 500 mL heptane:EtOAc, 2:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697862B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-4aca59d911b546eba2289e6708a6a0d2 |
| Source note | uspto-grants-2014_04 |