Triethylamine → HCID 86070947, compound

HRID 2366523Notes

Reaction equation

HRID 2366523 reaction equation
[OH:1][CH2:2][C:3]1[O:7][C:6]([CH:8]=[O:9])=[CH:5][CH:4]=1.[CH3:10][S:11](Cl)(=[O:13])=[O:12].C(N(CC)CC)C>C(Cl)Cl>[CH3:10][S:11]([O:1][CH2:2][C:3]1[O:7][C:6]([CH:8]=[O:9])=[CH:5][CH:4]=1)(=[O:13])=[O:12]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 2373325-(Hydroxymethyl)furfural

Product 1

HCID 86070947HCID 86070947, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Prepared by reacting 5-(hydroxymethyl)-2-furan-carboxaldehyde with methanesulfonic acid chloride in the presence of triethylamine in methylene chloride at ambient temperature. The crude product is further reacted without any more purification.

Workup

  1. customPrepared
  2. customat ambient temperature

Sources & evidence

ORD record
ord-1efa29d6b7e841cc9c9c7ba36a8502a1
Source dataset
uspto-grants-2014_04
Patent number
US08697868B2

Reaction notes

Loading…