HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69506827, compound → HCID 57457840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69506827 | HCID 69506827 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Product | HCID 57457840 | HCID 57457840 | — |
Reaction Steps
The method described in Part D of Example 64 was used to hydrogenate (35 psi, 2.4×105 Pa) ethyl 1-{[(3-nitroquinolin-4-yl)amino]methyl}cyclobutanecarboxylate (10.0 g, 30.4 mmol) in the presence of 5% platinum on carbon (1.0 g) to provide ethyl 1-{[(3-aminoquinolin-4-yl)amino]methyl}cyclobutanecarboxylate as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697873B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-e6447617a5954461be238b76ae71e464 |
| Source note | uspto-grants-2014_04 |