HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → N,N-DIETHYL-1-METHYL-PIPERIDINE-4-CARBOXAMIDE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-Methylpiperidine-4-carboxylic acid | HCID 2736939 | — |
| Reactant | Lasmiditan | HCID 11610526 | — |
| Product | N,N-DIETHYL-1-METHYL-PIPERIDINE-4-CARBOXAMIDE | HCID 412858 | — |
Reaction Steps
The present invention relates to a process for preparing 2,4,6-trifluoro-N-[6-(1-methyl-piperidine-4-carbonyl)-pyridin-2-yl]-benzamide or salt thereof, further comprising the step of: reacting 1-methylpiperidine-4-carboxylic acid with thionyl chloride and diethyl amine to yield N,N-diethyl-1-methylpiperidine-4-carboxamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08697876B2 |
| Source dataset | uspto-grants-2014_04 |
| ORD ID | ord-10810a44372647769ef5b4cf3ebc9bf3 |
| Source note | uspto-grants-2014_04 |