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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2367020Generated: October 31, 2026

Hydrochloric Acid → HCID 69005136, compound

https://huagongshe.com/reaction/2367020

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57803349HCID 57803349—
SolventDichloromethaneHCID 6344—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 69005136HCID 69005136—

Reaction Steps

To a solution of the intermediate of step E in methylene chloride (5 mL) was added 4 M HCl in dioxane (5 mL). After stirred at room temperature for 2 h, the resulting solution was concentrated in vacuo to give the HCl salt (350 mg) of the amine as a white solid. LCMS: (M+H)+ 364.4.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08697870B2
Source datasetuspto-grants-2014_04
ORD IDord-91e3559248554126ad7bdeead9fd30d7
Source noteuspto-grants-2014_04