HRID2367208

反应详情

EQUATION

反应方程式

HRID 2367208 的结构方程式

PROCEDURE

实验过程

The title compound was prepared following the General Procedure A using: (3,5-difluoro-4-formylphenyl)boronic acid (2.54 g, 13.7 mmol) and 6-chloro-N4-ethyl-2,4-pyrimidinediamine (2.36 g, 13.7 mmol). The solid was triturated with EtOAc and filtered to afford the title compound (1.63 g, 43%) as a yellow solid. LC-MS (ES) m/z=279 [M+H]+.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customThe solid was triturated with EtOAc
  3. filtrationfiltered