Hydrochloric Acid → Hydrochloric Acid

Participants

Reaction Steps

1,1-Dimethylethyl(2S,5R)-2-[(cyclohexylamino)carbonyl]-5-ethyl-4-morpholinecarboxylate (0.2963 g, 0.870 mmol) was taken up in HCl in 1,4-dioxane (4 M, 5 ml, 165 mmol) and stirred at room temperature overnight. The reaction was concentrated to afford a HCl salt of the title compound (0.256 g). LC-MS (ES) m/z=241 [M+H]+.

Provenance & Evidence